Reverse microemulsion mediated synthesis and characterization of lanthanum oxalate nanoparticles

ADVANCED NANOMATERIALS AND ITS APPLICATIONS
8-9th August, 2008 School of Materials Science & Nanotechnology,Jadavpur University


Reverse microemulsion mediated synthesis and characterization of lanthanum oxalate nanoparticles
Smritimoy Pramanik and Subhash Chandra Bhattacharya
Department of Chemistry, Jadavpur University, Kolkata – 700032, India.
*E-mail : scbhattacharyya@chemistry.jdvu.ac.in / sbjuchem@yahoo.com
Phone No: 033 2414 6223; Fax: 91(033) 24146584.
Abstract
Well-characterized, monodispersed biomimicking nanocavities formed by Aerosol OT (AOT) reverse micelle in H2O/ AOT / heptane at ω =10 (ω = [H2O]/[Surfactant]) was implemented to prepare Lanthanum oxalate (LaOx) nanoparticles employing intermixing of two microemulsions technique. The formed nanoparticles of LaOx have been characterized by the UV-visible, Transmission Electron Microscopy (TEM) as well as by Fourier Transformed Infrared (FTIR) spectroscopy. UV-visible and FTIR spectroscopic measurements confirm the formation of LaOx nanoparticles. TEM measurements show that the reverse micellar entrapped nanoparticles were spherical in shape.










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